Indentation + User defined profile Max load : 1000.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 20.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 1000.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 20.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 0.00 mN Loading rate : 100.00 mN/min Date : 14-04-16 Time : 09:19:02 Method : Oliver & Pharr Cycle n° 1 + Main results Hv= 15.101 Vickers H= 148.14 MPa E= 11.583 GPa + Hypothesis Poisson= 0.30 + Additional results Pm= 999.74 mN Hm= 2820.87 nm S= 1.1182 mN/nm Hc= 2152.84 nm Ht= 1926.82 nm H0= 1489.42 nm m= 1.54 Epsilon= 0.75 Ac= 6748784128.00 nm² Cycle n° 2 + Main results Hv= 14.987 Vickers H= 147.03 MPa E= 11.987 GPa + Hypothesis Poisson= 0.30 + Additional results Pm= 1009.47 mN Hm= 2851.83 nm S= 1.1651 mN/nm Hc= 2190.30 nm Ht= 1985.43 nm H0= 1699.05 nm m= 1.37 Epsilon= 0.76 Ac= 6865949184.00 nm² Cycle n° 3 + Main results Hv= 0.23502 Vickers H= 2.3055 MPa E= 3.6249 GPa + Hypothesis Poisson= 0.30 + Additional results Pm= 10.25 mN Hm= 1444.57 nm S= 0.2946 mN/nm Hc= 1417.29 nm Ht= 1409.77 nm H0= 1403.27 nm m= 1.24 Epsilon= 0.78 Ac= 4446237184.00 nm² Measured values Time (s) Pd (nm) Fn (mN) 0 0 0 0 0 0.2882 35.6829 0.5096 0 0 0.5764 69.5114 1.2081 0 0 0.8647 799.3768 30.2688 0 0 1.1529 1023.2762 56.8526 0 0 1.4411 1185.1481 86.557 0 0 1.7293 1303.717 116.6033 0 0 2.0175 1395.6014 146.6297 0 0 2.3057 1481.094 176.668 0 0 2.594 1530.0721 196.5928 0 0 2.8822 1597.251 226.6768 0 0 3.1704 1659.5223 256.8678 0 0 3.4586 1720.1383 286.4102 0 0 3.7468 1775.1082 316.6363 0 0 4.0351 1834.5272 346.3561 0 0 4.3233 1886.012 376.6862 0 0 4.6115 1935.9541 406.2793 0 0 4.8997 1969.9946 426.4897 0 0 5.1879 2015.615 456.3604 0 0 5.4761 2075.0012 486.5486 0 0 5.7644 2117.3982 516.3414 0 0 6.0526 2167.155 546.4334 0 0 6.3408 2210.2942 576.5254 0 0 6.629 2256.6492 606.657 0 0 6.9172 2300.2976 636.4483 0 0 7.2054 2329.0886 656.6296 0 0 7.4937 2374.5889 686.3004 0 0 7.7819 2412.0818 716.5571 0 0 8.0701 2449.7749 746.1042 0 0 8.3583 2499.7717 776.6768 0 0 8.6465 2535.8787 806.5505 0 0 8.9348 2574.03 836.5722 0 0 9.223 2614.2881 866.774 0 0 9.5112 2655.459 896.5256 0 0 9.7994 2678.2073 916.8961 0 0 10.0876 2715.9514 946.6935 0 0 10.3758 2753.3789 976.3764 0 0 10.6641 2785.866 1003.1375 0 0 10.9523 2791.4758 999.7133 0 0 11.2405 2794.248 1000.3787 0 0 11.5287 2801.4365 999.8186 0 0 11.8169 2804.2161 1000.6045 0 0 12.1052 2808.7053 1000.0323 0 0 12.3934 2809.2183 1000.6213 0 0 12.6816 2811.1392 1000.4869 0 0 12.9698 2806.0132 1000.3527 0 0 13.258 2813.8821 1000.4183 0 0 13.5462 2812.1467 1000.3771 0 0 13.8345 2810.1968 1000.4687 0 0 14.1227 2814.0132 1000.197 0 0 14.4109 2814.7043 1000.5923 0 0 14.6991 2814.9116 1000.2596 0 0 14.9873 2814.8462 1000.342 0 0 15.2756 2813.9258 1000.5037 0 0 15.5638 2817.2363 1000.1146 0 0 15.852 2822.5151 1000.5129 0 0 16.1402 2821.7437 1000.2184 0 0 16.4284 2817.7092 1000.4839 0 0 16.7166 2821.2715 1000.2687 0 0 17.0049 2820.1321 1000.4 0 0 17.2931 2821.8057 1000.0978 0 0 17.5813 2825.8511 1000.5892 0 0 17.8695 2820.354 1000.0018 0 0 18.1577 2821.2454 1000.2719 0 0 18.446 2821.0852 1000.2993 0 0 18.7342 2826.5313 1000.2504 0 0 19.0224 2824.3523 1000.8181 0 0 19.3106 2821.0525 1000.2001 0 0 19.5988 2822.5369 1000.3848 0 0 19.887 2820.7798 1000.548 0 0 20.1753 2824.5232 1000.5145 0 0 20.4635 2826.8987 1000.197 0 0 20.7517 2819.2153 1000.4183 0 0 21.0399 2819.6265 1000.2474 0 0 21.3281 2820.8997 1000.3069 0 0 21.6163 2819.0952 1000.3609 0 0 21.9046 2819.6375 1000.2871 0 0 22.1928 2823.2935 1000.2078 0 0 22.481 2826.7495 1000.6426 0 0 22.7692 2828.303 1000.2962 0 0 23.0574 2824.7778 1000.6838 0 0 23.3457 2822.2932 1000.4016 0 0 23.6339 2835.3462 1000.0841 0 0 23.9221 2830.8589 1000.4494 0 0 24.2103 2824.5742 1000.2093 0 0 24.4985 2834.3347 1000.072 0 0 24.7867 2822.093 1000.2199 0 0 25.075 2823.6245 1000.1849 0 0 25.3632 2831.1406 1000.2917 0 0 25.6514 2825.24 1000.3695 0 0 25.9396 2820.325 1000.2855 0 0 26.2278 2826.4963 1000.2587 0 0 26.5161 2824.2151 1000.3813 0 0 26.8043 2827.8337 1000.374 0 0 27.0925 2826.0476 999.9452 0 0 27.3807 2824.9016 1000.5297 0 0 27.6689 2820.7471 1000.4366 0 0 27.9571 2819.27 1000.4687 0 0 28.2454 2824.1848 1000.2581 0 0 28.5336 2823.1226 1000.4869 0 0 28.8218 2826.5857 1000.314 0 0 29.11 2819.0845 1000.3237 0 0 29.3982 2824.6177 1000.0796 0 0 29.6865 2821.8784 1000.4748 0 0 29.9747 2825.2144 1000.3237 0 0 30.2629 2821.46 1000.6243 0 0 30.5511 2821.5254 1000.5129 0 0 30.8393 2821.7109 1000.4045 0 0 31.1275 2822.3069 1000.2556 0 0 31.4158 2824.8147 1000.3965 0 0 31.704 2821.5801 1000.5327 0 0 31.9922 2820.3867 1000.4321 0 0 32.2804 2826.1167 1000.5037 0 0 32.5686 2826.3022 1000.3863 0 0 32.8568 2826.324 1000.3206 0 0 33.1451 2817.9094 1000.3161 0 0 33.4333 2822.0032 1000.4799 0 0 33.7215 2826.6584 1000.4307 0 0 34.0097 2821.6165 1000.2733 0 0 34.2979 2820.1685 1000.342 0 0 34.5862 2822.395 1000.2627 0 0 34.8744 2823.3772 1000.3664 0 0 35.1626 2815.3445 1000.3344 0 0 35.4508 2819.6191 1000.4397 0 0 35.739 2820.3113 1000.3271 0 0 36.0272 2817.1968 1000.2572 0 0 36.3155 2823.4705 1000.3925 0 0 36.6037 2823.3555 1000.3924 0 0 36.8919 2823.188 1000.6258 0 0 37.1801 2820.4995 1000.1391 0 0 37.4683 2820.8088 1000.1803 0 0 37.7566 2827.4373 1000.3466 0 0 38.0448 2827.3862 1000.3939 0 0 38.333 2828.4058 1000.4228 0 0 38.6212 2826.9822 1000.1359 0 0 38.9094 2822.0313 1000.455 0 0 39.1976 2826.3059 1000.3024 0 0 39.4859 2826.5132 1000.4274 0 0 39.7741 2827.2954 1000.1086 0 0 40.0623 2820.8816 1000.4397 0 0 40.3505 2823.4863 1000.5571 0 0 40.6387 2821.8899 1000.2726 0 0 40.927 2815.3044 1000.3939 0 0 41.2152 2822.4053 1000.6943 0 0 41.5034 2820.667 1000.3634 0 0 41.7916 2821.1616 1000.4183 0 0 42.0798 2825.0579 1000.6136 0 0 42.368 2817.8474 1000.2672 0 0 42.6563 2820.8743 1000.4122 0 0 42.9445 2820.4255 1000.2867 0 0 43.2327 2824.4985 1000.3657 0 0 43.5209 2824.324 1000.1182 0 0 43.8091 2821.7109 1000.5266 0 0 44.0974 2824.0212 1000.5511 0 0 44.3856 2818.2185 1000.4656 0 0 44.6738 2822.7441 1000.6075 0 0 44.962 2827.6482 1000.6639 0 0 45.2502 2829.0671 1000.2322 0 0 45.5384 2823.4705 1000.468 0 0 45.8267 2817.9111 1000.29 0 0 46.1149 2820.0105 1000.6164 0 0 46.4031 2819.2881 1000.5876 0 0 46.6913 2827.1389 1000.2535 0 0 46.9795 2819.5391 1000.5098 0 0 47.2677 2819.3027 1000.5541 0 0 47.556 2822.5732 1000.2612 0 0 47.8442 2824.5774 1000.4349 0 0 48.1324 2819.2805 1000.4138 0 0 48.4206 2824.6936 1000.2801 0 0 48.7088 2828.0667 1000.5984 0 0 48.9971 2823.9629 1000.5632 0 0 49.2853 2827.4954 1000.2672 0 0 49.5735 2822.657 1000.3787 0 0 49.8617 2824.323 1000.2672 0 0 50.1499 2821.0981 1000.3521 0 0 50.4381 2825.2417 1000.1248 0 0 50.7264 2818.6162 1000.5675 0 0 51.0146 2821.9299 1000.1156 0 0 51.3028 2821.1436 1000.8364 0 0 51.591 2828.4595 1000.5221 0 0 51.8792 2824.6941 1000.2108 0 0 52.1675 2825.5054 1000.3329 0 0 52.4557 2822.1125 1000.3819 0 0 52.7439 2817.3118 1000.2128 0 0 53.0321 2818.0159 1000.54 0 0 53.3203 2816.9021 1000.4487 0 0 53.6085 2827.1716 1000.2886 0 0 53.8968 2818.6843 1000.6624 0 0 54.185 2814.7444 1000.6487 0 0 54.4732 2818.5859 1000.1177 0 0 54.7614 2823.7957 1000.3375 0 0 55.0496 2821.5417 1000.4658 0 0 55.3379 2819.0142 1000.2985 0 0 55.6261 2824.2993 1000.42 0 0 55.9143 2822.0654 999.4815 0 0 56.2025 2818.8552 1000.4443 0 0 56.4907 2820.6086 1000.3572 0 0 56.7789 2817.3201 1000.4443 0 0 57.0672 2819.4883 1000.4702 0 0 57.3554 2818.4314 1000.2602 0 0 57.6436 2821.7932 1000.3955 0 0 57.9318 2818.1887 1000.2344 0 0 58.22 2817.3491 1000.7412 0 0 58.5083 2817.4436 1000.3604 0 0 58.7965 2816.0793 1000.5876 0 0 59.0847 2816.6396 1000.4885 0 0 59.3729 2821.6782 1000.5511 0 0 59.6611 2821.0579 1000.3515 0 0 59.9493 2820.3564 1000.0479 0 0 60.2376 2821.2693 1000.3884 0 0 60.5258 2822.6423 1000.4537 0 0 60.814 2825.4937 1000.2503 0 0 61.1022 2819.7102 1000.2017 0 0 61.3904 2820.8015 1000.7616 0 0 61.6786 2821.3435 1000.1284 0 0 61.9669 2826.3738 1000.5588 0 0 62.2551 2821.6462 1000.2656 0 0 62.5433 2817.8606 1000.5236 0 0 62.8315 2820.885 1000.2252 0 0 63.1197 2820.7317 1000.3448 0 0 63.408 2818.917 1000.0781 0 0 63.6962 2816.4287 1000.7296 0 0 63.9844 2823.1116 1000.4916 0 0 64.2726 2815.9739 1000.3527 0 0 64.5608 2824.5876 1000.0997 0 0 64.849 2821.2559 1000.309 0 0 65.1373 2821.3186 1000.5765 0 0 65.4255 2822.2837 1000.6569 0 0 65.7137 2820.386 1000.4786 0 0 66.0019 2820.5032 1000.0002 0 0 66.2901 2822.2749 1000.4672 0 0 66.5784 2820.9106 1000.0917 0 0 66.8666 2826.0522 1000.3802 0 0 67.1548 2823.0181 1000.3928 0 0 67.443 2821.092 1000.2477 0 0 67.7312 2826.1824 1000.2178 0 0 68.0194 2821.8967 1000.2117 0 0 68.3077 2820.8669 1000.2596 0 0 68.5959 2824.123 1000.6045 0 0 68.8841 2824.0867 1000.4931 0 0 69.1723 2824.25 1000.3446 0 0 69.4605 2820.6243 1000.418 0 0 69.7488 2817.5039 1000.2377 0 0 70.037 2820.2932 1000.279 0 0 70.3252 2824.1887 1000.197 0 0 70.6134 2820.8669 999.7392 0 0 70.9016 2819.9429 973.0454 0 0 71.1898 2788.7146 936.2412 0 0 71.4781 2779.4851 915.8936 0 0 71.7663 2744.5603 885.9161 0 0 72.0545 2721.3718 855.7693 0 0 72.3427 2694.7419 825.6348 0 0 72.6309 2673.4524 795.5322 0 0 72.9192 2638.5242 765.6569 0 0 73.2074 2610.9338 735.3483 0 0 73.4956 2582.8887 705.5524 0 0 73.7838 2551.9404 675.4072 0 0 74.072 252...
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